Information card for entry 7025188

Structure parameters

• Formula: C30 H32 Al2 Cl4 N2 O P2
• Calculated formula: C30 H32 Al2 Cl4 N2 O P2
• Title of publication: Reactivity of Zn(II), Mg(II) and Al(III) chlorides with a phosphinimine ligand: new tetrameric inverse crown ether structures.
• Authors of publication: Valerio Cárdenas, Cintya; Muñoz Hernández, Miguel Angel; Grévy, Jean-Michel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 28
• Pages of publication: 6441 - 6448
• a: 8.433 ± 0.0015 Å
• b: 9.7126 ± 0.0017 Å
• c: 11.539 ± 0.002 Å
• α: 91.184 ± 0.003°
• β: 94.033 ± 0.003°
• γ: 111.992 ± 0.003°
• Cell volume: 873 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.047
• Residual factor for significantly intense reflections: 0.0417
• Weighted residual factors for significantly intense reflections: 0.1213
• Weighted residual factors for all reflections included in the refinement: 0.1254
• Goodness-of-fit parameter for all reflections included in the refinement: 0.955
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No