Information card for entry 7025202

Structure parameters

• Formula: K10 O108 P4 Sb4 W26
• Calculated formula: K10 O108 P4 Sb4 W26
• Title of publication: Coordination between [H2P2W12O48]12- and antimony(III): synthesis and characterization of sandwich complex derived from the new {P2W13O51} fragment.
• Authors of publication: Zhang, Chun-Dan; Liu, Shu-Xia; Ma, Feng-Ji; Tan, Rui-Kang; Zhang, Wei; Su, Zhong-Min
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 34
• Pages of publication: 8033 - 8037
• a: 18.283 ± 0.006 Å
• b: 22.241 ± 0.006 Å
• c: 18.687 ± 0.006 Å
• α: 90°
• β: 102.684 ± 0.005°
• γ: 90°
• Cell volume: 7413 ± 4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0882
• Residual factor for significantly intense reflections: 0.0747
• Weighted residual factors for significantly intense reflections: 0.1814
• Weighted residual factors for all reflections included in the refinement: 0.1874
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No