Information card for entry 7025203

Structure parameters

• Formula: C36 H30 B Cl Fe N17 Ni O8
• Calculated formula: C36 H30 B Cl Fe N17 Ni O8
• Title of publication: An S = 3 cyanide-bridged tetranuclear Fe(III)(2)Ni(II)(2) square that exhibits slow relaxation of magnetization: synthesis, structure and magnetic properties.
• Authors of publication: Wu, Dayu; Zhang, Yanjuan; Huang, Wei; Sato, Osamu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 23
• Pages of publication: 5500 - 5503
• a: 12.812 ± 0.003 Å
• b: 14.131 ± 0.003 Å
• c: 14.936 ± 0.003 Å
• α: 69.05 ± 0.03°
• β: 68.8 ± 0.03°
• γ: 85.95 ± 0.03°
• Cell volume: 2349.1 ± 1.1 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1173
• Residual factor for significantly intense reflections: 0.1077
• Weighted residual factors for significantly intense reflections: 0.2673
• Weighted residual factors for all reflections included in the refinement: 0.2763
• Goodness-of-fit parameter for all reflections included in the refinement: 1.171
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No