Information card for entry 7025983

Structure parameters

• Formula: C64.5 H68 Li2 Nd O9.13 Si4
• Calculated formula: C64.5 H68 Li2 Nd O9.125 Si4
• Title of publication: Encapsulation of cyclooctatetraenyl dianion in an unusual organic/inorganic lanthanide triple-decker sandwich complex.
• Authors of publication: Lorenz, Volker; Blaurock, Steffen; Hrib, Cristian G.; Edelmann, Frank T.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 29
• Pages of publication: 6629 - 6631
• a: 29.533 ± 0.006 Å
• b: 39.637 ± 0.008 Å
• c: 42.832 ± 0.009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 50139 ± 18 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 70
• Hermann-Mauguin space group symbol: F d d d :2
• Hall space group symbol: -F 2uv 2vw
• Residual factor for all reflections: 0.1164
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.0997
• Weighted residual factors for all reflections included in the refinement: 0.115
• Goodness-of-fit parameter for all reflections included in the refinement: 0.792
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No