Crystallography Open Database

Information card for entry 7025983

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Coordinates	7025983.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64.5 H68 Li2 Nd O9.13 Si4
Calculated formula	C64.5 H68 Li2 Nd O9.125 Si4
Title of publication	Encapsulation of cyclooctatetraenyl dianion in an unusual organic/inorganic lanthanide triple-decker sandwich complex.
Authors of publication	Lorenz, Volker; Blaurock, Steffen; Hrib, Cristian G.; Edelmann, Frank T.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	29
Pages of publication	6629 - 6631
a	29.533 ± 0.006 Å
b	39.637 ± 0.008 Å
c	42.832 ± 0.009 Å
α	90°
β	90°
γ	90°
Cell volume	50139 ± 18 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	70
Hermann-Mauguin space group symbol	F d d d :2
Hall space group symbol	-F 2uv 2vw
Residual factor for all reflections	0.1164
Residual factor for significantly intense reflections	0.045
Weighted residual factors for significantly intense reflections	0.0997
Weighted residual factors for all reflections included in the refinement	0.115
Goodness-of-fit parameter for all reflections included in the refinement	0.792
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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