Information card for entry 7025984

Structure parameters

• Formula: C52 H152 B4 K4 O4 Si16
• Calculated formula: C52 H152 B4 K4 O4 Si16
• Title of publication: The quest for silylhydroboranes: (Me(3)Si)(3)SiBH(2).
• Authors of publication: Arp, Henning; Marschner, Christoph; Baumgartner, Judith
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 39
• Pages of publication: 9270 - 9274
• a: 14.291 ± 0.003 Å
• b: 26.47 ± 0.005 Å
• c: 51.562 ± 0.01 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 19505 ± 7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1301
• Residual factor for significantly intense reflections: 0.1045
• Weighted residual factors for significantly intense reflections: 0.2082
• Weighted residual factors for all reflections included in the refinement: 0.2212
• Goodness-of-fit parameter for all reflections included in the refinement: 1.221
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No