Crystallography Open Database

Information card for entry 7025985

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Coordinates	7025985.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C198 H438 B10 K10 Si52 Ti6
Calculated formula	C198 H438 B10 K10 Si52 Ti6
Title of publication	The quest for silylhydroboranes: (Me(3)Si)(3)SiBH(2).
Authors of publication	Arp, Henning; Marschner, Christoph; Baumgartner, Judith
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	39
Pages of publication	9270 - 9274
a	14.835 ± 0.003 Å
b	21.47 ± 0.004 Å
c	28.542 ± 0.006 Å
α	109.5 ± 0.03°
β	93.11 ± 0.03°
γ	97.9 ± 0.03°
Cell volume	8439 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1983
Residual factor for significantly intense reflections	0.1286
Weighted residual factors for significantly intense reflections	0.3167
Weighted residual factors for all reflections included in the refinement	0.3567
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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