Information card for entry 7026431

Structure parameters

• Formula: C22 H58 P2 Pd Si5
• Calculated formula: C22 H58 P2 Pd Si5
• SMILES: [Si]1(C(CCC1([Si](C)(C)C)[Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)=[Pd]([P](C)(C)C)[P](C)(C)C
• Title of publication: Synthesis and structures of (dialkylsilylene)bis(phosphine)-nickel, palladium, and platinum complexes and (η(6)-arene)(dialkylsilylene)nickel complexes.
• Authors of publication: Watanabe, Chieko; Inagawa, Yuichiro; Iwamoto, Takeaki; Kira, Mitsuo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 39
• Pages of publication: 9414 - 9420
• a: 9.596 ± 0.003 Å
• b: 11.341 ± 0.003 Å
• c: 16.777 ± 0.005 Å
• α: 78.74 ± 0.008°
• β: 82.334 ± 0.009°
• γ: 78.477 ± 0.008°
• Cell volume: 1746.1 ± 0.9 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0316
• Residual factor for significantly intense reflections: 0.0248
• Weighted residual factors for significantly intense reflections: 0.064
• Weighted residual factors for all reflections included in the refinement: 0.0664
• Goodness-of-fit parameter for all reflections included in the refinement: 0.992
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No