Information card for entry 7027006

Structure parameters

• Formula: C57 H49 Cl5 N2 O4 P4 Pd2 S
• Calculated formula: C57 H49 Cl5 N2 O4 P4 Pd2 S
• Title of publication: Arylsulfonylnitrene and arenesulfonyl azide complexes of palladium
• Authors of publication: Foch, Isabella; Párkányi, László; Besenyei, Gábor; Simándi, László I.; Kálmán, Alajos
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 3
• Pages of publication: 293
• a: 12.827 ± 0.001 Å
• b: 19.622 ± 0.001 Å
• c: 23.149 ± 0.006 Å
• α: 90°
• β: 98.74 ± 0.02°
• γ: 90°
• Cell volume: 5758.7 ± 1.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1618
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.1046
• Weighted residual factors for all reflections included in the refinement: 0.1201
• Goodness-of-fit parameter for all reflections included in the refinement: 0.909
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MOka
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No