Information card for entry 7027007

Structure parameters

• Formula: C60.5 H51.5 Cl3.5 N O3.67 P4 Pd2 S
• Calculated formula: C60.5 H51.5 Cl3.501 N O3.6695 P4 Pd2 S
• Title of publication: Arylsulfonylnitrene and arenesulfonyl azide complexes of palladium
• Authors of publication: Foch, Isabella; Párkányi, László; Besenyei, Gábor; Simándi, László I.; Kálmán, Alajos
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 3
• Pages of publication: 293
• a: 21.714 ± 0.004 Å
• b: 14.489 ± 0.003 Å
• c: 38.342 ± 0.007 Å
• α: 90°
• β: 90.39 ± 0.01°
• γ: 90°
• Cell volume: 12063 ± 4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1604
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.0915
• Weighted residual factors for all reflections included in the refinement: 0.1092
• Goodness-of-fit parameter for all reflections included in the refinement: 0.813
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MOkα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No