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Information card for entry 7027159
Preview
Coordinates | 7027159.cif |
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Original paper (by DOI) | HTML |
Formula | C64 H61 B Cl2 I O P3 W |
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Calculated formula | C64 H59 B Cl2 I O P3 W |
Title of publication | Cationic linear triphos, L [PhP(CH2CH2PPh2)2], alkyne complexes of molybdenum(II) and tungsten(II); crystal structures of [WI(CO)(L-P,P′,P ″)(η2-MeC2Me)]2[W6O19], [WI(CO)(L-P,P ′,P ″)(η2-MeC2Me)][BPh4] and [MoBr2(O){Ph2P(CH2)2PPh(CH2)2POPh2-P,P ′,O}] |
Authors of publication | Baker, Paul K.; Drew, Michael G. B.; Meehan, Margaret M. |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 1999 |
Journal issue | 5 |
Pages of publication | 765 |
a | 16.76 ± 0.02 Å |
b | 18.88 ± 0.02 Å |
c | 20.21 ± 0.02 Å |
α | 90° |
β | 109.913 ± 0.01° |
γ | 90° |
Cell volume | 6013 ± 11 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1149 |
Residual factor for significantly intense reflections | 0.0704 |
Weighted residual factors for significantly intense reflections | 0.1981 |
Weighted residual factors for all reflections included in the refinement | 0.2271 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.099 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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