Information card for entry 7027251

Structure parameters

• Formula: C51 H47 Cl F6 O P4 Pd
• Calculated formula: C51 H39 Cl F6 O P4 Pd
• Title of publication: Heterobimetallic alkoxysilyl cationic complexes: investigations into the displacement of a μ-η2-Si,O bridge by functional phosphine ligands
• Authors of publication: Blin, Joël; Braunstein, Pierre; Fischer, Jean; Kickelbick, Guido; Knorr, Michael; Morise, Xavier; Wirth, Tobias
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 13
• Pages of publication: 2159
• a: 11.5 ± 0.003 Å
• b: 20.814 ± 0.006 Å
• c: 21.055 ± 0.006 Å
• α: 90°
• β: 97.92 ± 0.02°
• γ: 90°
• Cell volume: 4992 ± 2 ų
• Cell temperature: 294 K
• Ambient diffraction temperature: 294 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.127
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for all reflections: 0.139
• Weighted residual factors for all reflections included in the refinement: 0.08
• Goodness-of-fit parameter for all reflections: 2.681
• Goodness-of-fit parameter for all reflections included in the refinement: 1.528
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No