Information card for entry 7027252

Structure parameters

• Formula: C54 H54 Cl8 O3 P4 Pd2
• Calculated formula: C54 H50 Cl8 O3 P4 Pd2
• Title of publication: Heterobimetallic alkoxysilyl cationic complexes: investigations into the displacement of a μ-η2-Si,O bridge by functional phosphine ligands
• Authors of publication: Blin, Joël; Braunstein, Pierre; Fischer, Jean; Kickelbick, Guido; Knorr, Michael; Morise, Xavier; Wirth, Tobias
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 13
• Pages of publication: 2159
• a: 21.171 ± 0.006 Å
• b: 21.171 ± 0.006 Å
• c: 14.309 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6413 ± 3 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 76
• Hermann-Mauguin space group symbol: P 41
• Hall space group symbol: P 4w
• Residual factor for all reflections: 0.046
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for all reflections: 0.073
• Weighted residual factors for all reflections included in the refinement: 0.054
• Goodness-of-fit parameter for all reflections: 1.607
• Goodness-of-fit parameter for all reflections included in the refinement: 1.181
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No