Information card for entry 7027271

Structure parameters

• Chemical name: 1,5,9-triphenyl-1,5,9-triphosphacyclododecane molybdenum tricarbonyl complex
• Formula: C30 H33 Mo O3 P3
• Calculated formula: C30 H33 Mo O3 P3
• Title of publication: The template synthesis of triaryl functionalised 1,5,9-triphosphacyclododecane on molybdenum using organocopper reagents †
• Authors of publication: Jones, David J.; Edwards, Peter G.; Tooze, Robert P.; Albers, Thomas
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 7
• Pages of publication: 1045
• a: 9.399 ± 0.004 Å
• b: 17.59 ± 0.03 Å
• c: 34.22 ± 0.02 Å
• α: 90°
• β: 90.15 ± 0.03°
• γ: 90°
• Cell volume: 5658 ± 10 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0833
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for significantly intense reflections: 0.085
• Weighted residual factors for all reflections included in the refinement: 0.0924
• Goodness-of-fit parameter for all reflections included in the refinement: 0.805
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No