Information card for entry 7027272

Structure parameters

• Formula: C16 H20 F6 O3.5 P Pd0.5 Se2
• Calculated formula: C32 H40 F12 O7 P2 Pd Se4
• Title of publication: Structural and complexation properties of diselenacrown ethers. Synthesis and crystal structure of a novel cationic palladium tetraselena complex
• Authors of publication: Bornet, C.; Amardeil, R.; Meunier, P.; Daran, J. C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 7
• Pages of publication: 1039
• a: 13.8454 ± 0.001 Å
• b: 15.9185 ± 0.0015 Å
• c: 19.7817 ± 0.0013 Å
• α: 90°
• β: 95.472 ± 0.007°
• γ: 90°
• Cell volume: 4340 ± 0.6 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.0489
• Goodness-of-fit parameter for significantly intense reflections: 1.0725
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No