Information card for entry 7027295

Structure parameters

• Formula: C25 H20 O15 Os6 S2
• Calculated formula: C25 H20 O15 Os6 S2
• Title of publication: Synthesis, structural characterization and reactivities of hexaosmium carbonyl clusters with six-membered cyclic thioether and thioxane ligands
• Authors of publication: Leung, Kelvin Sze-Yin; Wong, Wing-Tak
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 12
• Pages of publication: 2077
• a: 20.998 ± 0.001 Å
• b: 15.341 ± 0.002 Å
• c: 21.779 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7015.7 ± 1.2 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.0511
• Goodness-of-fit parameter for significantly intense reflections: 1.495
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No