Information card for entry 7027296

Structure parameters

• Formula: C20 H10 O15 Os5 S
• Calculated formula: C20 H10 O15 Os5 S
• Title of publication: Synthesis, structural characterization and reactivities of hexaosmium carbonyl clusters with six-membered cyclic thioether and thioxane ligands
• Authors of publication: Leung, Kelvin Sze-Yin; Wong, Wing-Tak
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 12
• Pages of publication: 2077
• a: 9.062 ± 0.001 Å
• b: 16.484 ± 0.002 Å
• c: 18.892 ± 0.002 Å
• α: 90°
• β: 94.76 ± 0.01°
• γ: 90°
• Cell volume: 2812.3 ± 0.6 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0453
• Weighted residual factors for significantly intense reflections: 0.0528
• Goodness-of-fit parameter for significantly intense reflections: 1.489
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No