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Information card for entry 7027307
Preview
Coordinates | 7027307.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25 H54 K N4 P Si2 |
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Calculated formula | C25 H54 K N4 P Si2 |
SMILES | [K]123(P(C([Si](C)(C)C)[Si](C)(C)C)c4c(cccc4)C[N]1(C)C)[N](C)(C)CC[N]2(C)CC[N]3(C)C |
Title of publication | Monomeric alkali metal complexes of a sterically demanding, donor-functionalised secondary phosphide ligand |
Authors of publication | Clegg, William; Doherty, Simon; Izod, Keith; Kagerer, Hartmut; O’Shaughnessy, Paul; Sheffield, Joanne M. |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 1999 |
Journal issue | 11 |
Pages of publication | 1825 |
a | 10.174 ± 0.0002 Å |
b | 28.7226 ± 0.0006 Å |
c | 12.1761 ± 0.0003 Å |
α | 90° |
β | 108.877 ± 0.001° |
γ | 90° |
Cell volume | 3366.77 ± 0.13 Å3 |
Cell temperature | 160 ± 2 K |
Ambient diffraction temperature | 160 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0815 |
Residual factor for significantly intense reflections | 0.0447 |
Weighted residual factors for significantly intense reflections | 0.0921 |
Weighted residual factors for all reflections included in the refinement | 0.1058 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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