Zirconium mixed ligand isopropoxide/aminoalkoxide complexes: crystal structures of [Zr2(OPri)6(L)2] and [Zr2(OBut)3(bdmap)4(OH)] {where L = dmap, 1-dimethylaminopropan-2-olate and bdmap, 1,1-bis(dimethylamino)propan-2-olate}
Authors of publication
Fleeting, Kirsty A.; O’Brien, Paul; Jones, Anthony C.; Otway, David J.; White, Andrew J. P.; Williams, David J.
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
1999
Journal issue
16
Pages of publication
2853
a
10.1455 ± 0.0009 Å
b
12.4123 ± 0.0011 Å
c
17.585 ± 0.002 Å
α
104.847 ± 0.009°
β
92.927 ± 0.01°
γ
113.762 ± 0.008°
Cell volume
1929 ± 0.4 Å3
Cell temperature
203 ± 2 K
Ambient diffraction temperature
203 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0569
Residual factor for significantly intense reflections
0.038
Weighted residual factors for all reflections
0.0949
Weighted residual factors for significantly intense reflections
0.085
Goodness-of-fit parameter for all reflections
1.041
Goodness-of-fit parameter for significantly intense reflections
