Zirconium mixed ligand isopropoxide/aminoalkoxide complexes: crystal structures of [Zr2(OPri)6(L)2] and [Zr2(OBut)3(bdmap)4(OH)] {where L = dmap, 1-dimethylaminopropan-2-olate and bdmap, 1,1-bis(dimethylamino)propan-2-olate}
Authors of publication
Fleeting, Kirsty A.; O’Brien, Paul; Jones, Anthony C.; Otway, David J.; White, Andrew J. P.; Williams, David J.
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
1999
Journal issue
16
Pages of publication
2853
a
22.066 ± 0.0015 Å
b
12.3385 ± 0.0009 Å
c
32.591 ± 0.003 Å
α
90°
β
101.162 ± 0.007°
γ
90°
Cell volume
8705.4 ± 1.2 Å3
Cell temperature
203 ± 2 K
Ambient diffraction temperature
203 ± 2 K
Number of distinct elements
5
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0694
Residual factor for significantly intense reflections
0.0537
Weighted residual factors for all reflections
0.148
Weighted residual factors for significantly intense reflections
0.1363
Goodness-of-fit parameter for all reflections
1.054
Goodness-of-fit parameter for significantly intense reflections
