New P–S–N containing ring systems. Reaction of 2,4-(naphthalene-1,8-diyl)-1,3,2,4-dithiadiphosphetane 2,4-disulfide with methylbis(trimethylsilyl)amine
Authors of publication
Kilián, Petr; Marek, Jaromír; Marek, Radek; Tousek, Jaromír; Humpa, Otakar; Slawin, Alexandra M. Z.; Touzín, Jirí; Novosad, Josef; Woollins, J. Derek
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
1999
Journal issue
13
Pages of publication
2231
a
9.8665 ± 0.0007 Å
b
10.4165 ± 0.0008 Å
c
17.1308 ± 0.0015 Å
α
105.217 ± 0.008°
β
102.994 ± 0.007°
γ
90.777 ± 0.006°
Cell volume
1650.4 ± 0.2 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0539
Residual factor for significantly intense reflections
0.0466
Weighted residual factors for all reflections
0.1288
Weighted residual factors for significantly intense reflections
0.1196
Goodness-of-fit parameter for all reflections
1.01
Goodness-of-fit parameter for significantly intense reflections
