Information card for entry 7027391

Structure parameters

• Formula: C33 H62 As P
• Calculated formula: C33 H62 As P
• SMILES: [As](CP([C@H]1[C@@H](CC[C@H](C1)C)C(C)C)[C@H]1[C@@H](CC[C@H](C1)C)C(C)C)(C1CCCCC1)C1CCCCC1
• Title of publication: A new synthetic route to ligands of the general composition R2PCH2ER′2 (E = P, As) and some rhodium complexes derived thereof
• Authors of publication: Wolf, Justin; Manger, Matthias; Schmidt, Ulrich; Fries, Guido; Barth, Dietmar; Weberndörfer, Birgit; Vicic, David A.; Jones, William D.; Werner, Helmut
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 11
• Pages of publication: 1867
• a: 10.064 ± 0.0004 Å
• b: 10.064 ± 0.0004 Å
• c: 57.716 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5062.5 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 152
• Hermann-Mauguin space group symbol: P 31 2 1
• Hall space group symbol: P 31 2"
• Residual factor for all reflections: 0.0729
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for all reflections: 0.0955
• Weighted residual factors for all reflections included in the refinement: 0.0854
• Goodness-of-fit parameter for all reflections: 0.927
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No