Information card for entry 7027432

Structure parameters

• Formula: C14 H22 As Li O2
• Calculated formula: C14 H21 As Li O2
• Title of publication: A metallated primary arsine; synthesis and structure of [PhAsHLi·2thf ]\ιnfty
• Authors of publication: Beswick, Michael A.; Lawson, Yvonne G.; Raithby, Paul R.; Wood, Jody A.; Wright, Dominic S.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 12
• Pages of publication: 1921
• a: 8.15 ± 0.002 Å
• b: 8.564 ± 0.002 Å
• c: 11.278 ± 0.002 Å
• α: 90°
• β: 101.87 ± 0.03°
• γ: 90°
• Cell volume: 770.3 ± 0.3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1293
• Residual factor for significantly intense reflections: 0.104
• Weighted residual factors for significantly intense reflections: 0.2339
• Weighted residual factors for all reflections included in the refinement: 0.2439
• Goodness-of-fit parameter for all reflections included in the refinement: 1.595
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No