Information card for entry 7027467

Structure parameters

• Formula: C12 H24 O5 Os
• Calculated formula: C12 O5 Os
• Title of publication: Preparation and crystal structures of oxoosmium(VI) diolato complexes
• Authors of publication: Lehtonen, Ari; Jokela, Jukka; Edwards, Peter G.; Sillanpää, Reijo
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 16
• Pages of publication: 2785
• a: 10.251 ± 0.003 Å
• b: 10.251 Å
• c: 7.283 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 765.3 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 4
• Space group number: 102
• Hermann-Mauguin space group symbol: P 42 n m
• Hall space group symbol: P 4n -2n
• Residual factor for all reflections: 0.0521
• Residual factor for significantly intense reflections: 0.0244
• Weighted residual factors for significantly intense reflections: 0.0548
• Weighted residual factors for all reflections included in the refinement: 0.061
• Goodness-of-fit parameter for all reflections included in the refinement: 1.097
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No