Information card for entry 7027468

Structure parameters

• Formula: C54 H77 O8 Os P
• Calculated formula: C54 H77 O8 Os P
• SMILES: [Os]12(=O)(OC3(CCCCC3)C3(O1)CCCCC3)OC1(CCCCC1)C1(O2)CCCCC1.P(=O)(c1ccccc1)(c1ccccc1)c1ccccc1.OC1(CCCCC1)C1(O)CCCCC1
• Title of publication: Preparation and crystal structures of oxoosmium(VI) diolato complexes
• Authors of publication: Lehtonen, Ari; Jokela, Jukka; Edwards, Peter G.; Sillanpää, Reijo
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 16
• Pages of publication: 2785
• a: 15.055 ± 0.005 Å
• b: 15.899 ± 0.008 Å
• c: 12.677 ± 0.005 Å
• α: 107.08 ± 0.04°
• β: 96.18 ± 0.03°
• γ: 112.9 ± 0.03°
• Cell volume: 2586 ± 2 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0656
• Residual factor for significantly intense reflections: 0.0357
• Weighted residual factors for significantly intense reflections: 0.0697
• Weighted residual factors for all reflections included in the refinement: 0.0768
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No