Information card for entry 7027541

Structure parameters

• Formula: C43.5 H43 Cl5 O6 P2 Rh2
• Calculated formula: C43.5 H43 Cl5 O6 P2 Rh2
• Title of publication: A new structural type of dinuclear rhodium(II) compounds: synthesis by serendipity and design; catalytic behaviour in carbene transfer reactions †
• Authors of publication: Estevan, Francisco; García-Bernabé, Abel; García-Granda, Santiago; Lahuerta, Pascual; Moreno, Eduardo; Pérez-Prieto, Julia; Sanaú, Mercedes; Ubeda, M. Angeles
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 19
• Pages of publication: 3493
• a: 17.9125 ± 0.001 Å
• b: 13.0427 ± 0.0008 Å
• c: 19.6074 ± 0.0012 Å
• α: 90°
• β: 94.89 ± 0.001°
• γ: 90°
• Cell volume: 4564.2 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0952
• Residual factor for significantly intense reflections: 0.0768
• Weighted residual factors for all reflections: 0.2031
• Weighted residual factors for significantly intense reflections: 0.1895
• Goodness-of-fit parameter for all reflections: 1.09
• Goodness-of-fit parameter for significantly intense reflections: 1.136
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No