Information card for entry 7027602

Structure parameters

• Formula: C48 H54 Li3 N3
• Calculated formula: C48 H54 Li3 N3
• Title of publication: Structural studies of the chiral lithium amides [{PhC(H)Me}2NLi] and [PhCH2{PhC(H)Me}NLi·THF] derived from α-methylbenzylamine †
• Authors of publication: Armstrong, David R.; Henderson, Kenneth W.; Kennedy, Alan R.; Kerr, William J.; Mair, Francis S.; Moir, Jennifer H.; Moran, Paul H.; Snaith, Ronald
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 22
• Pages of publication: 4063
• a: 19.66 ± 0.01 Å
• b: 20.414 ± 0.007 Å
• c: 10.185 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4088 ± 3 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1116
• Residual factor for significantly intense reflections: 0.0703
• Weighted residual factors for all reflections: 0.0864
• Weighted residual factors for significantly intense reflections: 0.0754
• Goodness-of-fit parameter for significantly intense reflections: 1.913
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No