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Information card for entry 7027603
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Coordinates | 7027603.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C38 H48 Li2 N2 O2 |
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Calculated formula | C38 H47 Li2 N2 O2 |
Title of publication | Structural studies of the chiral lithium amides [{PhC(H)Me}2NLi] and [PhCH2{PhC(H)Me}NLi·THF] derived from α-methylbenzylamine † |
Authors of publication | Armstrong, David R.; Henderson, Kenneth W.; Kennedy, Alan R.; Kerr, William J.; Mair, Francis S.; Moir, Jennifer H.; Moran, Paul H.; Snaith, Ronald |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 1999 |
Journal issue | 22 |
Pages of publication | 4063 |
a | 16.55 ± 0.005 Å |
b | 19.729 ± 0.005 Å |
c | 10.455 ± 0.0013 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3413.7 ± 1.4 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.1747 |
Residual factor for significantly intense reflections | 0.0654 |
Weighted residual factors for significantly intense reflections | 0.1711 |
Weighted residual factors for all reflections included in the refinement | 0.2136 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.045 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7027603.html
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