Information card for entry 7027659

Structure parameters

• Formula: C23 H21 Mo N2 O4 P
• Calculated formula: C23 H21 Mo N2 O4 P
• Title of publication: A convenient method for selective substitutions at the backbone of a co-ordinated imidazolylphosphine P‒N ligand. Single crystal X-ray analyses of [Mo(CO)4(MeImCH2PPh2)] and its ethyl substituted derivative [Mo(CO)4(MeImCHEtPPh2)] †
• Authors of publication: Jalil, M. Abdul; Fujinami, Shuhei; Nishikawa, Hiroaki
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 19
• Pages of publication: 3499
• a: 11.453 ± 0.001 Å
• b: 10.396 ± 0.002 Å
• c: 19.428 ± 0.002 Å
• α: 90°
• β: 93.33 ± 0.01°
• γ: 90°
• Cell volume: 2309.3 ± 0.5 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0269
• Weighted residual factors for significantly intense reflections: 0.0445
• Goodness-of-fit parameter for significantly intense reflections: 1.008
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No