Information card for entry 7027660

Structure parameters

• Formula: C18 H29 Cl N4 Ni O5 S2
• Calculated formula: C18 H29 Cl N4 Ni O5 S2
• Title of publication: Nickel(II)-induced activation of a carbon‒nitrogen single bond(s) of a co-ordinated ligand by hydroxylated substrates: generation of mono- and bi-nuclear complexes with modified ligand frameworks †
• Authors of publication: Bhattacharyya, Sudeep; Ghosh, Dipesh; Endo, Akira; Shimizu, Kunio; Weakley, Timothy J. R.; Chaudhury, Muktimoy
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 21
• Pages of publication: 3859
• a: 11.779 ± 0.004 Å
• b: 13.233 ± 0.003 Å
• c: 14.732 ± 0.003 Å
• α: 90°
• β: 100.03 ± 0.02°
• γ: 90°
• Cell volume: 2261.2 ± 1 ų
• Cell temperature: 294.2 K
• Ambient diffraction temperature: 294 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.044
• Weighted residual factors for significantly intense reflections: 0.045
• Goodness-of-fit parameter for significantly intense reflections: 1.8
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No