Information card for entry 7027785

Structure parameters

• Formula: C30 H60 Cl2 Mg2 O2 P2
• Calculated formula: C30 H60 Cl2 Mg2 O2 P2
• Title of publication: A convenient synthetic route to substituted phosphavinyl Grignard reagents: synthesis and characterisation of [{RPC(But)MgX(OEt2)}2] (R = cyclohexyl, cyclopentyl, ethyl or mesityl; X = Cl or Br) †
• Authors of publication: Hibbs, David E.; Jones, Cameron; Richards, Anne F.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 20
• Pages of publication: 3531
• a: 11.6149 ± 0.0005 Å
• b: 12.441 ± 0.0007 Å
• c: 15.8853 ± 0.0004 Å
• α: 72.073 ± 0.003°
• β: 70.757 ± 0.003°
• γ: 65.849 ± 0.003°
• Cell volume: 1937.23 ± 0.16 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0995
• Residual factor for significantly intense reflections: 0.0545
• Weighted residual factors for significantly intense reflections: 0.1299
• Weighted residual factors for all reflections included in the refinement: 0.1462
• Goodness-of-fit parameter for all reflections included in the refinement: 0.991
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No