Information card for entry 7027844

Structure parameters

• Formula: C40 H54 Cl2 Mo N2 O3
• Calculated formula: C43 H45 Cl2 Mo N2 O3
• Title of publication: Molybdenum‒carbon functionalities supported by a quadridentate Schiff-base ligand: the reactivity of trans-dichloro[N,N′-bis(salicylidene)-o-phenylenediaminato]molybdenum(IV) ‡
• Authors of publication: Solari, Euro; Maltese, Cristiano; Latronico, Mario; Floriani, Carlo; Chiesi-Villa, Angiola; Rizzoli, Corrado
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 14
• Pages of publication: 2395
• a: 13.648 ± 0.003 Å
• b: 15.105 ± 0.005 Å
• c: 11.149 ± 0.003 Å
• α: 108.48 ± 0.03°
• β: 105.37 ± 0.02°
• γ: 63.91 ± 0.02°
• Cell volume: 1936.3 ± 1 ų
• Cell temperature: 25 K
• Ambient diffraction temperature: 133 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0977
• Residual factor for significantly intense reflections: 0.0507
• Weighted residual factors for all reflections: 0.1426
• Weighted residual factors for significantly intense reflections: 0.1284
• Goodness-of-fit parameter for all reflections: 1.069
• Goodness-of-fit parameter for significantly intense reflections: 1.118
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKa
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No