Information card for entry 7027845

Structure parameters

• Formula: C47 H47 Mo N2 O2
• Calculated formula: C47 H47 Mo N2 O2
• Title of publication: Molybdenum‒carbon functionalities supported by a quadridentate Schiff-base ligand: the reactivity of trans-dichloro[N,N′-bis(salicylidene)-o-phenylenediaminato]molybdenum(IV) ‡
• Authors of publication: Solari, Euro; Maltese, Cristiano; Latronico, Mario; Floriani, Carlo; Chiesi-Villa, Angiola; Rizzoli, Corrado
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 14
• Pages of publication: 2395
• a: 9.188 ± 0.002 Å
• b: 30.228 ± 0.004 Å
• c: 13.615 ± 0.002 Å
• α: 90 ± 0°
• β: 103.99 ± 0.02°
• γ: 90 ± 0°
• Cell volume: 3669.2 ± 1.1 ų
• Cell temperature: 25 K
• Ambient diffraction temperature: 133 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.143
• Residual factor for significantly intense reflections: 0.0676
• Weighted residual factors for all reflections: 0.1956
• Weighted residual factors for significantly intense reflections: 0.1728
• Goodness-of-fit parameter for all reflections: 1.101
• Goodness-of-fit parameter for significantly intense reflections: 1.187
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKa
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No