Information card for entry 7027910

Structure parameters

• Formula: C48 H74 K2 N4 Si6
• Calculated formula: C48 H74 K2 N4 Si6
• SMILES: [K]123[N]4([Si](C)(C)C)C(c5ccccc5)=[N]1(C(=C([Si](C)(C)C)[Si](C)(C)C)c1ccccc1)[K]14[N]2([Si](C)(C)C)C(c2ccccc2)=[N]13C(=C([Si](C)(C)C)[Si](C)(C)C)c1ccccc1
• Title of publication: Metal (Li, K, SnII and HgII) complexes of the 1,3-diazaallyl [N(R)C(Ph)NC(Ph)CR2]− (R = SiMe3)
• Authors of publication: Hitchcock, Peter B.; Lappert, Michael F.; Layh, Marcus
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 18
• Pages of publication: 3113
• a: 9.227 ± 0.003 Å
• b: 18.05 ± 0.008 Å
• c: 16.192 ± 0.011 Å
• α: 90°
• β: 96.09 ± 0.04°
• γ: 90°
• Cell volume: 2682 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.09
• Residual factor for significantly intense reflections: 0.0561
• Weighted residual factors for all reflections: 0.1527
• Weighted residual factors for significantly intense reflections: 0.1319
• Goodness-of-fit parameter for all reflections: 1.043
• Goodness-of-fit parameter for significantly intense reflections: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No