Information card for entry 7028057

Structure parameters

• Formula: C52 H44 B2 Cl9 O4 P2 Rh
• Calculated formula: C52 H44 B2 Cl8.998 O4 P2 Rh
• Title of publication: Boron‒boron bond oxidative addition to rhodium(I) and iridium(I) centres
• Authors of publication: Clegg, William; Lawlor, Fiona J.; Marder, Todd B.; Nguyen, Paul; Norman, Nicholas C.; Orpen, A. Guy; Quayle, Michael J.; Rice, Craig R.; Robins, Edward G.; Scott, Andrew J.; Souza, Fabio E. S.; Stringer, Graham; Whittell, George R.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 2
• Pages of publication: 301
• a: 11.2003 ± 0.0006 Å
• b: 13.5606 ± 0.0007 Å
• c: 19.0819 ± 0.001 Å
• α: 83.551 ± 0.001°
• β: 83.064 ± 0.001°
• γ: 79.373 ± 0.001°
• Cell volume: 2815.6 ± 0.3 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0452
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for all reflections: 0.1022
• Weighted residual factors for significantly intense reflections: 0.0978
• Goodness-of-fit parameter for all reflections: 1.054
• Goodness-of-fit parameter for significantly intense reflections: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No