Information card for entry 7028402

Structure parameters

• Formula: C14 H14 Br2 N4 Pb
• Calculated formula: C14 H14 Br2 N4 Pb
• Title of publication: Mechanochemical solid state anion-exchange of lead(II) coordination polymers via an intermediate coordination polymer; new precursors for the preparation of PbBr2/Pb3O2Br2, PbBr(OH) and PbO nanoparticles.
• Authors of publication: Hashemi, Lida; Morsali, Ali; Joo, Sang Woo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 4
• Pages of publication: 1489 - 1492
• a: 15.179 ± 0.004 Å
• b: 4.2189 ± 0.001 Å
• c: 16.682 ± 0.003 Å
• α: 90°
• β: 117.679 ± 0.017°
• γ: 90°
• Cell volume: 946 ± 0.4 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.053
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.1077
• Weighted residual factors for all reflections included in the refinement: 0.1235
• Goodness-of-fit parameter for all reflections included in the refinement: 1.216
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No