Information card for entry 7028403

Structure parameters

• Formula: C28 H28 Br2.16 N9.84 O5.5 Pb2
• Calculated formula: C28 H28 Br2.164 N9.836 O5.508 Pb2
• Title of publication: Mechanochemical solid state anion-exchange of lead(II) coordination polymers via an intermediate coordination polymer; new precursors for the preparation of PbBr2/Pb3O2Br2, PbBr(OH) and PbO nanoparticles.
• Authors of publication: Hashemi, Lida; Morsali, Ali; Joo, Sang Woo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 4
• Pages of publication: 1489 - 1492
• a: 8.3995 ± 0.0001 Å
• b: 17.9496 ± 0.0003 Å
• c: 27.9998 ± 0.0005 Å
• α: 104.475 ± 0.001°
• β: 89.987 ± 0.001°
• γ: 117.915 ± 0.001°
• Cell volume: 3578.05 ± 0.11 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0651
• Residual factor for significantly intense reflections: 0.0346
• Weighted residual factors for significantly intense reflections: 0.0787
• Weighted residual factors for all reflections included in the refinement: 0.0926
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No