Information card for entry 7029230

Structure parameters

• Formula: C47 H61 P2
• Calculated formula: C47 H61 P2
• Title of publication: Secondary diphosphine and diphosphido ligands: synthesis, characterisation and group 1 coordination compounds.
• Authors of publication: Ritch, Jamie S.; Julienne, Delphine; Rybchinski, Shayne R.; Brockman, Kathryne S.; Johnson, Kevin R. D.; Hayes, Paul G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 1
• Pages of publication: 267 - 276
• a: 33.518 ± 0.003 Å
• b: 15.0365 ± 0.0013 Å
• c: 16.5961 ± 0.0015 Å
• α: 90°
• β: 97.155 ± 0.001°
• γ: 90°
• Cell volume: 8299.2 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 3
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0967
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1168
• Weighted residual factors for all reflections included in the refinement: 0.1401
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No