Information card for entry 7029231

Structure parameters

• Formula: C92 H152 K2 O18 P2
• Calculated formula: C84 H136 K2 O16 P2
• Title of publication: Secondary diphosphine and diphosphido ligands: synthesis, characterisation and group 1 coordination compounds.
• Authors of publication: Ritch, Jamie S.; Julienne, Delphine; Rybchinski, Shayne R.; Brockman, Kathryne S.; Johnson, Kevin R. D.; Hayes, Paul G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 1
• Pages of publication: 267 - 276
• a: 13.3096 ± 0.0019 Å
• b: 17.99 ± 0.003 Å
• c: 21.542 ± 0.003 Å
• α: 87.891 ± 0.002°
• β: 87.743 ± 0.002°
• γ: 68.936 ± 0.002°
• Cell volume: 4808.2 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1122
• Residual factor for significantly intense reflections: 0.0642
• Weighted residual factors for significantly intense reflections: 0.1624
• Weighted residual factors for all reflections included in the refinement: 0.1805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No