Information card for entry 7029778

Structure parameters

• Formula: C72 H74 Li2 N6 P2
• Calculated formula: C72 H74 Li2 N6 P2
• SMILES: [Li]12[N](c3c(C(C)C)cccc3C(C)C)=P(c3ccccc3)(c3ccccc3)N(c3ccccc3)[N]1(c1ccccc1)[Li]1[N](c3c(C(C)C)cccc3C(C)C)=P(c3ccccc3)(c3ccccc3)N(c3ccccc3)[N]12c1ccccc1
• Title of publication: Reactivity studies of a soluble LiH-complex and non-spectator behaviour of its stabilising phosphinoamide ligand.
• Authors of publication: Stasch, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 19
• Pages of publication: 7078 - 7086
• a: 14.562 ± 0.003 Å
• b: 14.076 ± 0.003 Å
• c: 14.694 ± 0.003 Å
• α: 90°
• β: 91.81 ± 0.03°
• γ: 90°
• Cell volume: 3010.4 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0685
• Residual factor for significantly intense reflections: 0.0486
• Weighted residual factors for significantly intense reflections: 0.1172
• Weighted residual factors for all reflections included in the refinement: 0.1275
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No