Information card for entry 7029890

Structure parameters

• Formula: C22 H42 Ag N8 O44 P W12
• Calculated formula: C22 H32 Ag N8 O44 P W12
• Title of publication: The key role of -CH3 steric hindrance in bis(pyrazolyl) ligand on polyoxometalate-based compounds.
• Authors of publication: Tian, Ai-Xiang; Yang, Yang; Ying, Jun; Li, Na; Lin, Xiao-Ling; Zhang, Ju-Wen; Wang, Xiu-Li
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 22
• Pages of publication: 8405 - 8413
• a: 12.863 ± 0.005 Å
• b: 12.959 ± 0.005 Å
• c: 19.517 ± 0.005 Å
• α: 80.885 ± 0.005°
• β: 89.984 ± 0.005°
• γ: 78.821 ± 0.005°
• Cell volume: 3149.7 ± 1.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1324
• Residual factor for significantly intense reflections: 0.0726
• Weighted residual factors for significantly intense reflections: 0.1637
• Weighted residual factors for all reflections included in the refinement: 0.1892
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No