Information card for entry 7029891

Structure parameters

• Formula: C66 H101 Ag6 N24 O40 P W12
• Calculated formula: C66 H96 Ag6 N24 O40 P W12
• Title of publication: The key role of -CH3 steric hindrance in bis(pyrazolyl) ligand on polyoxometalate-based compounds.
• Authors of publication: Tian, Ai-Xiang; Yang, Yang; Ying, Jun; Li, Na; Lin, Xiao-Ling; Zhang, Ju-Wen; Wang, Xiu-Li
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 22
• Pages of publication: 8405 - 8413
• a: 14.1484 ± 0.0014 Å
• b: 14.2546 ± 0.0015 Å
• c: 16.6307 ± 0.0016 Å
• α: 72.529 ± 0.002°
• β: 72.936 ± 0.002°
• γ: 61.456 ± 0.002°
• Cell volume: 2765.1 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1145
• Residual factor for significantly intense reflections: 0.0802
• Weighted residual factors for significantly intense reflections: 0.1669
• Weighted residual factors for all reflections included in the refinement: 0.18
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No