Information card for entry 7030111

Structure parameters

• Formula: C18 H20 K N3
• Calculated formula: C18 H20 K N3
• Title of publication: Lithium, sodium and potassium picolyl complexes: syntheses, structures and bonding.
• Authors of publication: Kennedy, Alan R.; Mulvey, Robert E.; Urquhart, Robert I.; Robertson, Stuart D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 38
• Pages of publication: 14265 - 14274
• a: 7.24604 ± 0.00012 Å
• b: 12.9546 ± 0.0002 Å
• c: 17.9978 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1689.45 ± 0.05 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0383
• Residual factor for significantly intense reflections: 0.0316
• Weighted residual factors for significantly intense reflections: 0.0649
• Weighted residual factors for all reflections included in the refinement: 0.0679
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No