Information card for entry 7030112

Structure parameters

• Formula: C15 H29 Li N4
• Calculated formula: C15.012 H29 Li N4.002
• Title of publication: Lithium, sodium and potassium picolyl complexes: syntheses, structures and bonding.
• Authors of publication: Kennedy, Alan R.; Mulvey, Robert E.; Urquhart, Robert I.; Robertson, Stuart D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 38
• Pages of publication: 14265 - 14274
• a: 9.2329 ± 0.0016 Å
• b: 13.071 ± 0.003 Å
• c: 14.754 ± 0.002 Å
• α: 105.504 ± 0.016°
• β: 91.111 ± 0.013°
• γ: 96.93 ± 0.017°
• Cell volume: 1700.8 ± 0.6 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.138
• Residual factor for significantly intense reflections: 0.0823
• Weighted residual factors for significantly intense reflections: 0.2131
• Weighted residual factors for all reflections included in the refinement: 0.2749
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No