Information card for entry 7030218

Structure parameters

• Formula: C37 H40 N O4 P2 Si2 W
• Calculated formula: C37 H40 N O4 P2 Si2 W
• Title of publication: Synthesis and oxidation of d6 tungsten pincer complexes: a complete series of tungsten(II) hydridocarbonyl and halocarbonyl pincer complexes.
• Authors of publication: Wingard, Leah A.; White, Peter S.; Templeton, Joseph L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 37
• Pages of publication: 11438 - 11448
• a: 8.9073 ± 0.0003 Å
• b: 24.0432 ± 0.001 Å
• c: 17.5465 ± 0.0008 Å
• α: 90°
• β: 94.894 ± 0.003°
• γ: 90°
• Cell volume: 3744.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0634
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0692
• Weighted residual factors for all reflections included in the refinement: 0.0788
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No