Information card for entry 7030219

Structure parameters

• Formula: C34 H40 B Cl2 F4 N O3 P2 Si2 W
• Calculated formula: C34 H39 B Cl2 F4 N O3 P2 Si2 W
• Title of publication: Synthesis and oxidation of d6 tungsten pincer complexes: a complete series of tungsten(II) hydridocarbonyl and halocarbonyl pincer complexes.
• Authors of publication: Wingard, Leah A.; White, Peter S.; Templeton, Joseph L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 37
• Pages of publication: 11438 - 11448
• a: 13.1944 ± 0.0005 Å
• b: 18.9951 ± 0.0008 Å
• c: 15.4344 ± 0.0006 Å
• α: 90°
• β: 90.665 ± 0.002°
• γ: 90°
• Cell volume: 3868 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 10
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.091
• Residual factor for significantly intense reflections: 0.0623
• Weighted residual factors for significantly intense reflections: 0.1512
• Weighted residual factors for all reflections included in the refinement: 0.1649
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No