Information card for entry 7030768

Structure parameters

• Chemical name: [K(THF)2][C{N(2,6-iPr2C6H3)}2(CH)C]
• Formula: C35 H51 K N2 O2
• Calculated formula: C35 H51 K N2 O2
• Title of publication: Alkali metal salts of ditopic carbanionic carbenes as reagents for the synthesis of novel complexes of group 12 and 14 metals.
• Authors of publication: Waters, Jordan B.; Goicoechea, Jose M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 38
• Pages of publication: 14239 - 14248
• a: 10.8804 ± 0.0001 Å
• b: 14.4926 ± 0.0001 Å
• c: 21.7725 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3433.2 ± 0.05 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0649
• Residual factor for significantly intense reflections: 0.0548
• Weighted residual factors for significantly intense reflections: 0.1475
• Weighted residual factors for all reflections included in the refinement: 0.1564
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No