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Information card for entry 7030769
Preview
Coordinates | 7030769.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | [K(18-crown-6)(THF)2][{C[N(2,6-iPr2C6H3)]2(CH)C}2Pb[N(SiMe3)2]]*THF |
---|---|
Formula | C84 H136 K N5 O9 Pb Si2 |
Calculated formula | C84 H136 K N5 O9 Pb Si2 |
SMILES | [Pb](C1=CN([C]N1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C)(C1=CN([C]N1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C)N([Si](C)(C)C)[Si](C)(C)C.[K]12345([O]6CC[O]1CC[O]2CC[O]3CC[O]4CC[O]5CC6)([O]1CCCC1)[O]1CCCC1.O1CCCC1 |
Title of publication | Alkali metal salts of ditopic carbanionic carbenes as reagents for the synthesis of novel complexes of group 12 and 14 metals. |
Authors of publication | Waters, Jordan B.; Goicoechea, Jose M. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2014 |
Journal volume | 43 |
Journal issue | 38 |
Pages of publication | 14239 - 14248 |
a | 22.8186 ± 0.0001 Å |
b | 26.9545 ± 0.0002 Å |
c | 29.4392 ± 0.0002 Å |
α | 90° |
β | 90.504 ± 0.001° |
γ | 90° |
Cell volume | 18106.3 ± 0.2 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1023 |
Residual factor for significantly intense reflections | 0.0582 |
Weighted residual factors for significantly intense reflections | 0.1177 |
Weighted residual factors for all reflections included in the refinement | 0.1367 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.038 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7030769.html
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