Crystallography Open Database

Information card for entry 7030818

Preview

Coordinates	7030818.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H35 Li O4.5 Si
Calculated formula	C27.9996 H34.9992 Li O4.4997 Si
Title of publication	Crown ether adducts of light alkali metal triphenylsilyls: synthesis, structure and hydrosilylation catalysis.
Authors of publication	Leich, Valeri; Lamberts, Kevin; Spaniol, Thomas P.; Okuda, Jun
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	38
Pages of publication	14315 - 14321
a	11.9898 ± 0.0009 Å
b	11.9898 ± 0.0009 Å
c	21.5449 ± 0.0017 Å
α	90°
β	90°
γ	120°
Cell volume	2682.2 ± 0.4 Å³
Cell temperature	220 ± 2 K
Ambient diffraction temperature	220 ± 2 K
Number of distinct elements	5
Space group number	165
Hermann-Mauguin space group symbol	P -3 c 1
Hall space group symbol	-P 3 2"c
Residual factor for all reflections	0.1287
Residual factor for significantly intense reflections	0.0961
Weighted residual factors for significantly intense reflections	0.2733
Weighted residual factors for all reflections included in the refinement	0.3126
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7030818.html