Information card for entry 7030819

Structure parameters

• Formula: C30 H39 Na O5.5 Si
• Calculated formula: C29.9994 H38.9988 Na O5.4996 Si
• Title of publication: Crown ether adducts of light alkali metal triphenylsilyls: synthesis, structure and hydrosilylation catalysis.
• Authors of publication: Leich, Valeri; Lamberts, Kevin; Spaniol, Thomas P.; Okuda, Jun
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 38
• Pages of publication: 14315 - 14321
• a: 12.858 ± 0.005 Å
• b: 12.858 ± 0.005 Å
• c: 10.756 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 1540 ± 1.1 ų
• Cell temperature: 220 ± 2 K
• Ambient diffraction temperature: 220 ± 2 K
• Number of distinct elements: 5
• Space group number: 147
• Hermann-Mauguin space group symbol: P -3
• Hall space group symbol: -P 3
• Residual factor for all reflections: 0.1661
• Residual factor for significantly intense reflections: 0.1155
• Weighted residual factors for significantly intense reflections: 0.19
• Weighted residual factors for all reflections included in the refinement: 0.2141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No