Crystallography Open Database

Information card for entry 7032039

7032038 << 7032039 >> 7032040

Preview

Coordinates	7032039.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H41 Cl4 N2 Pd Sb
Calculated formula	C40 H41 Cl4 N2 Pd Sb
Title of publication	A new library of arsine, stibine-stabilized N-heterocyclic carbene palladium complexes: synthesis, structures and activities in C-C and C-N coupling reactions.
Authors of publication	Yang, Jin; Li, Pinhua; Zhang, Yicheng; Wang, Lei
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	37
Pages of publication	14114 - 14122
a	19.8365 ± 0.0019 Å
b	13.9429 ± 0.0013 Å
c	14.4872 ± 0.0014 Å
α	90°
β	91.925 ± 0.001°
γ	90°
Cell volume	4004.6 ± 0.7 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0349
Residual factor for significantly intense reflections	0.0277
Weighted residual factors for significantly intense reflections	0.0641
Weighted residual factors for all reflections included in the refinement	0.0687
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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